1 – Overview of CTC and PALs 10-23-11

May 12, 2018 | Author: Khoa Nam Nguyen | Category:Documents
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CTC Analyticals AG Support Training

Page 1

Introductions Name?

Where are you from? How long with Agilent/Channel Partner? Are you Service Engineer or other job?

Chemistry or Electronics background? Experience with GC, GC-MS, LC-LC-MS or CTC? How is your English?

1 – CTC-Agilent Overview Page 2

CTC Analyticals AG Support Training for GC, GC-MS LC, LC-MS using Multi Technique Chemstation MS Chemstation EZ Chrom OpenLab CDS Chemstation Edition OpenLab CDS EZChrom Edition Mass Hunter

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Where design meets performance…

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1 – CTC-Agilent Overview

CTC Sample Injection Technology Founded 1987 in Basel Switzerland Started with GC OEM Autosamplers Model A200S Pittcon 1996 Launch of PAL Systems Private owned ISO 9001 registered company

Dedicated to gas- and liquid handling systems Inhouse R&D and QC / Outsourced production No direct sales and marketing organisation All systems tested in house prior to shipment

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1 – CTC-Agilent Overview

Why CTC Autosamplers?

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1 – CTC-Agilent Overview

Multipurpose Injection System Liquid mode with large volume injection up to 500?l

Headspace without sample loop or heated transfer line SPME extraction for heated and agitated samples ITEX (In Tube Extraction) sample enrichment mode

Liquid Page 7

Headspace

SPME

NEW 1 – CTC-Agilent Overview

Sample Capacity

Sample capacity up to:

600 1ml vials 294 2ml vials 96 10ml vials 96 20ml vials 8 96 well microplates 8 384 well microplates 8 96 deepwell plates Page 8

1 – CTC-Agilent Overview

Sample Cooling Options

Tray Cooler 4°C – 70°C (Peltier version) 200 98

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1ml vials 2ml vials

Tray Cooler 2 4°C – 70°C (Peltier version)

200 1ml vials 98 2ml vials 32 10ml vials 32 20ml vials

1 – CTC-Agilent Overview

PAL Gas Chromatography Applications

Multi Purpose GC Injectors/Samplers for Gas Chromatography

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1 – CTC-Agilent Overview

GC-PAL and Combi-PAL Overview Injector 80

Mounting Hardware for 6850/6890/7890 Liquid Injections only, no upgrade Page 11

LHS2

Sampler 80 Sampler 120

Mounting Hardware for 6850/6890/7890 Upgrade Options for up to 4 different Sample Prep Injection Modes 1 – CTC-Agilent Overview

Non Upgradable Configuration Injector 80 Liquid mode standard configuration • 10?l syringe kit for liquid injection • 1 Tray for 98 2ml vials / 78 1ml vials • 1 WashStation for two different solvents and 1 standard liquid

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G6502-CTC

GC PAL, CTC Colors

G6502B

GC PAL, Agilent Injector 80, Agilent branded

1 – CTC-Agilent Overview

Upgradable Configurations Sampler 80

Liquid mode standard configuration (shipped with all Systems) • 10?l syringe kit for liquid injection • 1 Tray for 98 2ml vials / 78 1ml vials • 1 WashStation for two different solvents and 1 standard liquid Headspace mode standard configuration (Option 111, or G6503B) • 2.5 ml syringe kit with heated syringe holder

Sampler 120

• 1 Tray for 32 10 or 20ml vials

• 6 Position Heated Agitator

G6500-CTC

Combi-PAL w/ Headspace, CTC Colors

G6501-CTC

Combi-PAL w/o Headspace, CTC Colors

G6501B

Combi-PAL w/o Headspace, Agilent Sampler 80, Agilent branded

G6509-CTC

Combi-PAL 120 cm rail w/o Headspace, CTC Colors

G6509B

Combi-PAL 120 cm rail w/o HS, Agilent Sampler 120, Agilent branded

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1 – CTC-Agilent Overview

Model G6501B/G6509B ? Upgrade Path Liquid ? Headspace ? SPME

? ITEX

1. Starting with Liquid Injection (G6501B or G6509B) 2. Add Headspace Option (G6503B) 3. Add SPME (G6504B) 4. Add ITEX II (soon)

Liquid Syringe Page 14

HS Option

SPME Option

ITEX Traps 1 – CTC-Agilent Overview

Review: Three Basic GC Systems Liquid Injections Only, Non Upgradable, 80 cm X Rail GC-Pal, G6502-CTC, G6502B Agilent GC Injector 80

Liquid Injections, Supports Headspace, SPME & ITEX II, 80 cm Rail Combi-Pal, LHS0, LHS2, G6500-CTC, G6501-CTC, G6501B Agilent GC Sampler 80

Liquid Injections, Supports Headspace, SPME & ITEX II, 120 cm Rail LHSX, LHS9, G6509-CTC, G6509B Agilent GC Sampler 120 1 – CTC-Agilent Overview Page 15

PAL Liquid Chromatography Applications Liquid Chromatography

High Throughput LC Injectors

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1 – CTC-Agilent Overview

PAL Liquid Chromatography Systems

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1 – CTC-Agilent Overview

Entry Level System LC PAL

Fixed configuration no options available Sample Capacity 216 2ml vials 4 x 96/384 Deepwell plates 4 x 96/384 Shallow well plates Injection Valve Single 2 position 6-port valve Bench Space 50 cm width

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1 – CTC-Agilent Overview

Mid range System HTC PAL High Throughput Compact Flexible Configuration Max. Sample Capacity 648 2ml vials 12 96/384 Deepwell plates 24 96/384 Shallow well plates Cooled Sample Storage Option Max. Injection Valves One 2 position 6-port valve Optional 2 and 3 Valve Operation Multiposition Valve Drives Bench Space 50 cm width Page 19

1 – CTC-Agilent Overview

High Throughput System HTS PAL

High Throughput Standard Flexible Configuration Max. Sample Capacity 972 2ml vials 18 96/384 Deepwell plates 24 96/384 Shallow well plates Cooled Sample Storage Option Max. Injection Valves Two 2 position 6-port valves Optional 2 and 3 Valve Operation Multiposition Valve Drives PAL Dilutor Option Bench Space 80 cm width Page 20

1 – CTC-Agilent Overview

IFC PAL FractionCollector Prep Version Injection Side 98 2ml vials or 32 10/20ml vials Collection Side Tube sizes 1092pcs. 13x100mm (9ml) 700pcs. 16x100mm (12ml) 700pcs. 16x150mm (20ml) 504pcs. 18x150mm (27ml) 504pcs. 20x150mm (34ml) 294pcs. 25x150mm (55ml) optional Gilson 215 rack holder Injection / Wash 6-port VICI Valco prep valve up to 50ml/min 2 different wash solvents Injection volume up to 5‘000µl Page 21

1 – CTC-Agilent Overview

HPLC PAL‘s Injection volumes Syringes / CTC label 9 different Sizes

Size

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10?l 25?l 50?l 100?l 250?l 500?l 1000?l 2500?l

Injection range 1 – 10?l 2.5 – 25?l 5 – 50?l 10 – 10?l 25 – 250?l 50 – 500?l 100 – 1000?l 250 – 2500?l

5000?l

500 – 5000?l

1 – CTC-Agilent Overview

Sample Storage for HTS / HTC PAL

Trayholders

Trays 1/2/10/20ml Page 23

Microplate Stack

Tray 4°C – 70°C (Peltier Cooling)

Deepwell Stack

Stack 4°C – 40°C (Peltier Cooling) 1 – CTC-Agilent Overview

Agilent Products and Instrument Description

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1290 Infinity LC Injector HTC (G4278A)

1290 Infinity LC Injector HTS (G4277A)

• 50 cm wide • Up to 12 well plates cooled • 40 ppm or 0.004% typical carryover • Injection volume up to 100 μL with DLW, and up to 5 mL* with Fast wash

• 80 cm wide • Up to 24 well plates cooled • 40 ppm or 0.004% typical carryover • Injection volume up to 100 μL with DLW, and up to 5 mL* with Fast wash

1 – CTC-Agilent Overview

Review: LC Systems and Configurations HTC/HTS PAL High Throughput LC Injection Systems (20062010) 600 bar Injection valve, fast/active wash station, Generic Pal design HTC, G4270-CTC: 50cm, compact system, medium capacity HTS, G4271-CTC: 80cm, standard system, high capacity

1290 Infinity LC Injector HTS/HTC (since 2010) Proprietary 1200 bar Injection valve, Dynamic Load and Wash DLW, xtelectronics, faster cycles times, lower carryover, Agilent Design HTS, G4277A: 80cm, standard system, high capacity HTC, G4278A: 50cm, compact system, medium capacity

1 – CTC-Agilent Overview Page 25

GC PAL / Combi-PAL / HTS / HTC / LC PAL Local control Control by handheld terminal without PC (standalone contact closure remote start operation) Instrument access for Local setup and teach function Method parameters Sample List Utility Functions

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1 – CTC-Agilent Overview

Options

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1 – CTC-Agilent Overview

PAL Dilutor Option for HTS PAL External Dilutor module Feeds liquid directly through the injection syringe into samples Not compatible with DLW

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1 – CTC-Agilent Overview

PAL Barcode Reader (with B.01.0x only) Laser scanner reads barcode labels on 2, 10 and 20ml vials Transfers data into Sample List Requires steel caps for magnetic vial transport Barcode types UPC versions A and E EAN 8 and EAN 13 Code 39 Interleaved 2 of 5 Discrete 2 of 5 Code 128 Code 93 Codabar

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1 – CTC-Agilent Overview

PAL Option Flow Through Cell Online Analysis Application Stainless steel flow cell body Internal Volume 1ml Flow rate up to 100ml/min ¼ inch Swagelok connectors Sample aspiration through Teflon coated Septum Cleaning port for easy maintenance

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1 – CTC-Agilent Overview

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